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Analytical problems relating to the preparation and control of egg pasta: GC-FID analysis.<\/p>\n\t\t
2005<\/p>\n\t\t
Author(s)<\/p>\n\t\t
Daniele Naviglio - Fabiana Pizzolongo<\/p>\n\t\t
Caption<\/p>\n\t\t
GC chromatogram obtained by analysing lipids of egg-yolk after the addition of squalene as internal standard (SI)<\/p>\n\t\t
Comments<\/p>\n\t\t
This gas chromatogram was obtained by injecting one microliter of lipids extracted from egg-yolk on RTX-65 TG capillary column (Restek corp.) 30m lenght, 0.25 mm i.d., 0.1 micron f.t. PTV injector was programmed starting from 60 \u00b0C (6 sec.) increase 999 \u00b0C\/min to 370 \u00b0C held for two minutes. Column program was 250 \u00b0C (2 min.) increase 5\u00b0C\/min to 360 \u00b0C (2 min.)<\/p>\n\t\t
Discovery<\/p>\n\t\t
For the first time squalene as internal standard and polar column were used for cholesterol determination. Gas chromatogram allowed to accurately detect the number of eggs added to special pasta.<\/p>\n\t\t
Bibliography<\/p>\n\t\t
NAVIGLIO D., PIZZOLONGO F. (2006). Problematiche analitiche relative alla preparazione e al controllo delle paste all'uovo. Tecnica Molitoria, 57(2), 121-130.<\/p>\n\t\t
Email<\/p>\n\t\t
naviglio@unina.it<\/p>\n\t<\/div>\n<\/div>\n\n"}